cyclization

Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.

综述了二碘化钐在分子内化反应中应用。

Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.

以苯甲酰氯为原料,经酰化,还原,合等反应合成左旋西替利嗪盐酸盐,反应总收率为8.05%。

Method The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.

方法以克拉霉素为起始原料,经水解、乙酰化、碳酸酯化、化、脱碳酸酯化、酰化、氨基甲酸酯化和合等反应合成目标化合物。

Bromacil was synthesized using 2-bromobutane and urea as the starting materials in three steps including condensation,cyclization and bromination with total yield of 61%.

以2-溴丁烷和尿素作为起始原料,经缩合、化、溴代三步反应得到除草定,总收率为61%。

N butyl 2 ethoxy thioacridone was prepared from o chloro benzoic acid and p phenetidine by means of Ullman reaction,cyclization,N alkylation and sulfurization.

以邻氯苯甲酸和对乙基苯为原料,经过苯基化、二化、N-烷基化、硫代化反应合成了N-丁基-2-乙基硫代吖啶酮。

This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.

讨论了以草酸二乙酯为原料,经过克莱森缩合、合、氨解反应合成5甲基异唑3甲酰工艺改进。

In this paper, the synthesis of 2 - chloranthraquinone and 2 - aminoanthraquinone was studied.It was prepared from phthalic anhydride by acetyiation, hydrolysis and cyclization.

以苯酐和取代苯为原料,经过乙酰化、水解及合反应,合成了2-氯蒽醌和2-氨基蒽醌,并对影响收率工艺条件进行了研究。

Aqueous titanium trichloride promoted intermolecular reductive cyclization of 1,2 -diketone and o-nitroaniline in basic media provides a convenient method for the synthesis of quinoxaline derivatives.

本文研究了三氯化钛水溶液作用下,邻硝基苯与1,2-二酮在碱性介质中分子间成反应,提供了一个方便地合成取代喹喔啉类化合物方法。