Bromacil was synthesized using 2-bromobutane and urea as the starting materials in three steps including condensation,cyclization and bromination with total yield of 61%.
以2-溴丁烷和尿素作为起始原料,缩合、环化、溴代三步反应得到除草定,总收率为61%。
Bromacil was synthesized using 2-bromobutane and urea as the starting materials in three steps including condensation,cyclization and bromination with total yield of 61%.
以2-溴丁烷和尿素作为起始原料,缩合、环化、溴代三步反应得到除草定,总收率为61%。
The title resin has been prepared by Friedel-Crafts acylation followed by bromination and amination.The method avoids the utilization of cancerogenic chloromethyl methyl ether.
通过付氏酰基化反应引入酰基,接着溴化、胺化,得到标题树脂。该法避免了使用氯甲醚。
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